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1,1’-联萘-2,2’-二酚-单-[(-)-孟基]碳酸酯旋光异构体的反相高效液相色谱分离及光学纯度测定
Optical Isomeric Separation and Determination of (R,S)-1,1’-Binaphthalene-2,2’-Diol-Mono-[(-)-Menthyl] Carbonate by RP-HPLC

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1_1’_联萘_2_2’_二酚_单_[__孟基]碳酸酯旋光异构体的反相高效液相色.pdf (300.8Kb)
Date
2000-11
Author
阮源萍
陈安齐
刘文远
郑锦丽
黄培强
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  • 化学化工-已发表论文 [14235]
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Abstract
采用反相高效液相色谱法分离了 1 ,1’-联萘 - 2 ,2’-二酚 -单 [(- ) -孟基 ]碳酸酯旋光异构体 .考察了这一对旋光化合物的反相高效液相色谱行为 .结果表明 ,C1 8及 C8柱和醇 /水流动相体系适合于这一对旋光异构体的分离 .进一步优化了色谱分离条件 ,并用于它们的光学纯度测定。 R)1,1’inaphthalene2,2’diolmono[()menthyl] carbonate and (S)1,1’binaphthalene2,2’diolmono[()menthyl] carbonate were separated by reversephase high performance liquid chromatography . The effects of different types of stationary phase and mobile phase composition on the optical isomeric separation were investigated. The result showed that the C 18 or C 8 column and alcoholwater as mobile phase are suitable for the separation. The mechanism of separation is also discussed.
Citation
厦门大学学报(自然科学版),2000(6):803-807
URI
https://dspace.xmu.edu.cn/handle/2288/2945

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