Electrospray ionization mass spectrometry study on dipeptide 4-chlorobutyl ester produced from refluxing of amino acid with phosphoryl chloride in tetrahydrofuran
Date
2005-10Author
Gui Ji Zhou
Ze Liu
Tong Jian Wang
Peng Xiang Xu
Gou Tang
唐果
Yong Ye
Yu Fen Zhao
赵玉芬
Collections
- 化学化工-已发表论文 [14469]
Abstract
Phosphoryl chloride was able to promote the formation of peptide and the ringopening of tetrahydrofuran (THF) followed by a sequence of successive reactions by simply refluxing. ESI multistage tandem mass spectrometry was applied to trace the reaction and elucidate the product structures, dipeptide 4-chlorobutyl ester. Copyright (c) 2005 John Wiley & Sons, Ltd.